Beilstein J. Org. Chem.2010,6, 932–937, doi:10.3762/bjoc.6.104
, and were characterized by their spectroscopic data. The individual isomers can now be easily identified from their 1H NMR spectra even if only one of them is present.
Keywords: cyclophanes; diformyl[2.2]paracyclophanes; layeredcompounds; NMR spectroscopy; structure assignment; Introduction
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Graphical Abstract
Scheme 1:
Preparation of the four [2.2]paracyclophane dialdehydes 4 by cycloaddition (ps - pseudo).